Synthesis of some novel quinone diimine derivatives of benzo‐15‐crown‐5 for application in Hg2+ recognition
Luminescence2013Vol. 29(6), pp. 586–590
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S. D. Jagadale, Anand D. Sawant, Prasad Patil, D. R. Patil, Abhijeet G. Mulik, Dattatray Chandam, Sandeep Sankpal, M. B. Deshmukh
Abstract
A series of novel fluoroionophore bearing derivatives of benzo-15-crown-5 were synthesized by the amination of benzo-15-crown-5 followed by condensation with different quinones in the presence of titanium tetrachloride (TiCl4 ) and 1,4-diazabicyclo-[2.2.2]octane. The compounds were characterized by infrared, (1) H and (13) C nuclear magnetic resonance, mass spectroscopy and elemental analysis. Absorption and fluorescence spectral characteristics of these compounds were studied. It was observed that the anthraquinone derivative was acting as an Hg(2+) ion sensor.
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