Synthesis of Isolable Thiirane-2-thione (α-Dithiolactone) from Thioketene S-Oxide
Journal of the American Chemical Society2004Vol. 126(31), pp. 9508–9509
Citations Over TimeTop 10% of 2004 papers
Kentaro Okuma, Toshiyuki Shigetomi, Yoshinori Nibu, Kosei Shioji, Masato Yoshida, Yoshinobu Yokomori
Abstract
Reaction of di-tert-butyl thioketene S-oxide with Lawesson reagent gave 3,3-di-tert-butylthiirane-2-thione in 88% yield. Oxidation of thiirane-2-thione with m-chloroperbenzoic acid afforded 3,3-di-tert-butylthiirane-2-thione S-oxide. The reaction of thiirane-thione was described.
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