New Approach for Size- and Shape-Controlled Preparation of Pd Nanoparticles with Organic Ligands. Synthesis and Application in Catalysis
Journal of the American Chemical Society2007Vol. 129(23), pp. 7252–7253
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Valentine P. Ananikov, Nikolay V. Orlov, I. P. Beletskaya, Victor N. Khrustalev, Mikhail Yu. Antipin, Tatiana V. Timofeeva
Abstract
A novel approach was developed to prepare Pd nanoparticles with organic ligands in high yields. The structural unit of the Pd species was constructed involving Pd−S bonds. The synthesized Pd particles were highly selective catalysts of S−H bond addition to alkynes under microwave heating. An X-ray diffraction study of one of the products of the addition reaction revealed unusual supramolecular organization of cation/anion layers.
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