Formation of Nanoparticles by Intramolecular Cross-Linking: Following the Reaction Progress of Single Polymer Chains by Atomic Force Microscopy
Journal of the American Chemical Society2007Vol. 129(37), pp. 11350–11351
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Abstract
Aliphatic polycarbonates with pendant vinyl groups were transformed into nanoparticles through intramolecular olefin cross-metathesis under dilute conditions. Reaction progress was monitored by AFM, revealing a range of structures from extended linear molecules at 0% cross-linking to isolated particles at 76% cross-linking.
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