Radical Reduction of Aromatic Azides to Amines with Tributylgermanium Hydride
The Journal of Organic Chemistry2005Vol. 71(1), pp. 434–437
Citations Over TimeTop 14% of 2005 papers
Luisa Benati, Giorgio Bencivenni, Rino Leardini, Matteo Minozzi, Daniele Nanni, Rosanna Scialpi, Piero Spagnolo, Giuseppe Zanardi
Abstract
[reaction: see text] Aromatic azides are inert toward tributylgermanium hydride under thermal conditions in the absence and in the presence of a radical initiator but in the presence of catalytic amounts of benzenethiol undergo fast reaction, yielding reduced anilines and 2-germylated derivatives in high overall yields.
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