Radical Reduction of Aromatic Azides to Amines with Triethylsilane
The Journal of Organic Chemistry2006Vol. 71(15), pp. 5822–5825
Citations Over TimeTop 10% of 2006 papers
Luisa Benati, Giorgio Bencivenni, Rino Leardini, Matteo Minozzi, Daniele Nanni, Rosanna Scialpi, Piero Spagnolo, Giuseppe Zanardi
Abstract
Aromatic azides are inert toward triethylsilane under thermal conditions in the presence of a radical initiator, but in the presence of additional catalytic amounts of tert-dodecanethiol, they afford anilinosilanes and thence the corresponding anilines in virtually quantitative yields.
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