Acetyl Chloride–Silver Nitrate–Acetonitrile: A Reagent System for the Synthesis of 2-Nitroglycals and 2-Nitro-1-Acetamido Sugars from Glycals
The Journal of Organic Chemistry2011Vol. 76(14), pp. 5832–5837
Citations Over TimeTop 10% of 2011 papers
Abstract
A new reagent system comprising acetyl chloride, silver nitrate, and acetonitrile has been developed for the synthesis of 2-nitroglycals from the corresponding glycals. Under certain conditions, the formation of 2-nitro-1-acetamido sugars has also been observed. In addition, a few other non-carbohydrate-derived olefins also gave the corrresponding conjugated nitroolefins.
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