Structural Determination of the La@C82 Isomer
The Journal of Physical Chemistry B2001Vol. 105(15), pp. 2971–2974
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Takeshi Akasaka, Takatsugu Wakahara, Shigeru Nagase, Kaoru Kobayashi, Markus Waelchli, Kazunori Yamamoto, Masahiro Kondo, Shingo Shirakura, Yutaka Maeda, Tatsuhisa Kato, Masahiro Kako, Yasuhiro Nakadaira, Xiang Gao, Eric Van Caemelbecke, Karl M. Kadish
Abstract
A stable diamagnetic monoanion of the La@C82 isomer was electrochemically prepared and isolated in order to disclose its cage symmetry. By measuring the 13C NMR spectrum of the anion, it was determined for the first time that the isomer has Cs symmetry, as was also confirmed by density functional calculations.
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