Coupling of AlkynylTMS Derivatives with Vinylic Iodides. An Efficient Route to 1,3-Enynes and Dienes
Organic Letters2001Vol. 3(25), pp. 4107–4110
Citations Over TimeTop 15% of 2001 papers
Abstract
[reaction: see text] CuCl-promoted coupling of alkynylTMS derivatives with vinyl iodides leads to 1,3-enynes in high yield. Enynes prepared from homopropargylic alcohols undergo intramolecular hydrosilylation and subsequent silyl cleavage with TBAF to afford 1,3-dienes.
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