A General Method for the Formation of Aryl−Sulfur Bonds Using Copper(I) Catalysts
Organic Letters2002Vol. 4(16), pp. 2803–2806
Citations Over TimeTop 10% of 2002 papers
Abstract
[reaction: see text] We report a mild, palladium-free synthetic protocol for the cross-coupling reaction of aryl iodides and thiols using 10 mol % CuI and 10 mol % neocuproine, with NaOt-Bu as the base, in toluene at 110 degrees C. Using this protocol, we have shown that a variety of aryl sulfides can be synthesized in excellent yields from readily available iodides and thiols.
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