An Acid-Catalyzed Macrolactonization Protocol
Organic Letters2002Vol. 4(21), pp. 3743–3745
Citations Over TimeTop 10% of 2002 papers
Abstract
[reaction: see text] An efficient macrolactonization protocol devoid of any base was developed derived from the use of vinyl esters in transesterification. Subjecting a hydroxy acid and ethoxyacetylene to 2 mol % [RuCl(2)(p-cymene)](2) in toluene followed by addition of camphorsulfonic acid or inverse addition provided macrolactones in good yields.
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