Bleach/Acetic Acid-Promoted Chlorinative Ring Expansion of [2.2.1]- and [2.2.2]-Bicycles
Organic Letters2002Vol. 4(22), pp. 3899–3902
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Abstract
[formula: see text] Treatment of vinyl-substituted [2.2.1]- and [2.2.2]-bicyclocarbinols with NaOCl and AcOH provides [3.2.1]- and [3.2.2]-beta-chloro-bicycloketones, respectively. For [2.2.2]-bicycles, these chlorinative ring expansions are particularly efficient and selective.
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