Convergent Synthesis of the ABCDEF-Ring System of Yessotoxin and Adriatoxin
Organic Letters2002Vol. 4(22), pp. 3943–3946
Citations Over TimeTop 10% of 2002 papers
Abstract
[formula: see text] The convergent synthesis of the ABCDEF-ring system of yessotoxin and adriatoxin was accomplished. This efficient convergent strategy was performed on the basis of the coupling of the acetylide of the A-ring and the triflate of the DEF-ring, oxidation of the alkyne to diketone, intramolecular diacetalization, and stereoselective reduction of the diacetal with Et3SiH-TMSOTf.
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