Solid-Phase Total Synthesis of the Pentacyclic System Lamellarins U and L
Organic Letters2003Vol. 5(16), pp. 2959–2962
Citations Over TimeTop 10% of 2003 papers
Abstract
[reaction: see text] A total solid-phase synthesis of lamellarins U and L has been achieved. The conversion of an aldehyde group into a formate by a Baeyer-Villiger reaction and a intramolecular [3 + 2] cycloaddition of a 3,4-dihydroisoquinolinium salt over a triple bond comprise the key steps of the process. Each transformation has been controlled with the proper spectroscopic and analytical methods.
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