Synthesis of the C11−C29 Fragment of Amphidinolide F
Organic Letters2004Vol. 6(21), pp. 3865–3868
Citations Over TimeTop 10% of 2004 papers
Abstract
[reaction: see text] An efficient synthesis of the C(11)-C(29) fragment 31 of amphidinolide F has been accomplished via a diastereoselective [3 + 2]-annulation reaction of allylsilane 5 and ethyl glyoxylate to prepare the key tetrahydrofuran 15 and a highly stereoselective methyl ketone aldol reaction to generate the C(11)-C(16) segment.
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