Enantioselective Total Synthesis of (−)-Dehydrobatzelladine C
Organic Letters2004Vol. 6(8), pp. 1253–1255
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Abstract
The oxidation of two tethered Biginelli adducts was examined as a potential key step in total syntheses of highly oxidized batzelladine and crambescidin alkaloids. Although angular hydroxyl substitution could not be introduced, dehydrogenation was readily accomplished. This latter conversion is a key step in the first total synthesis of dehydrobatzelladine C. [structure: see text]
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