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A Practical Synthetic Method of O-(2-(Pyrazol-1-yl)pyridin-5-yl)methylhydroxylamine as a Component of Modithromycin | doi.page

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A Practical Synthetic Method of O-(2-(Pyrazol-1-yl)pyridin-5-yl)methylhydroxylamine as a Component of Modithromycin

Organic Process Research & Development·2011·Vol. 16(2), pp. 220–224

Sumio Shimizu, Toshikazu Hakogi, Naomi Umesako, Yutaka Yokota, T. Ueki

Abstract

A practical synthesis of O-(2-(pyrazol-1-yl)pyridin-5-yl)methylhydroxylamine was achieved from the inexpensive raw materials, 2-chloro-5-chloromethylpyridine, pyrazole, and acetone oxime, using common reagents such as aq NaOH and sulfuric acid.

Abstract

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