Using a novel plug flow reactor for the in situ, simultaneous, monitoring of SAXS and WAXD during crystallisation from solution
Physical Chemistry Chemical Physics2003Vol. 5(22), pp. 4998–4998
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H. Alison, Roger J. Davey, John Garside, Michael J. Quayle, G. J. T. Tiddy, David T. Clarke, Gareth R. Jones
Abstract
The design and application of a novel plug flow crystalliser is described. Simultaneous collection of SAXS and WAXD during the nucleation and crystal growth of a small organic molecule from solution is reported. Preliminary data imply the separation of a non-diffracting phase prior to the appearance of crystalline solid.
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