Solvent effect in a “solvent free” reaction
CrystEngComm2007Vol. 9(10), pp. 879–879
Citations Over TimeTop 10% of 2007 papers
Dario Braga, S.L. Giaffreda, Fabrizia Grepioni, Michele R. Chierotti, Roberto Gobetto, Giuseppe Palladino, M. Polito
Abstract
Vapour digestion of a mixture of solid [Fe(η5-C5H4–C5H4N)2] and solid pimelic acid HOOC(CH2)5COOH in the presence of solvent vapours generates co-crystals of different stoichiometry depending on the protic or aprotic nature of the solvent. The nature of the products has been ascertained by a combined use of SSNMR and X-ray diffraction.
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