Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding
Chemical Communications2010Vol. 46(40), pp. 7572–7572
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Kotaro Fujii, Ana Lazuen Garay, J. K. Hill, Elena Sbircea, Zhigang Pan, Mingcan Xu, David C. Apperley, Stuart L. James, Kenneth D. M. Harris
Abstract
Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal-organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.
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