Synthesis of Ar@C60 using molecular surgery
Chemical Communications2020Vol. 56(72), pp. 10521–10524
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Sally Bloodworth, Gary Hoffmann, Mark C. Walkey, George R. Bacanu, Julie Herniman, Malcolm H. Levitt, Richard J. Whitby
Abstract
Synthesis of Ar@C60 is described, using a route in which high-pressure argon filling of an open-fullerene and photochemical desulfinylation are the key steps for >95% encapsulation of the noble gas. Enrichment by recycling HPLC leads to quantitative incorporation of argon in the product endofullerene, with a mass recovery of tens of milligrams, allowing the first characterisation of fine structure in the solution 13C NMR spectrum.
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