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Spin trapping azidyl (N3•), cyanatyl (OCN•), cyanyl (•CN) radicals, and chlorine atom (Cl•)
Canadian Journal of Chemistry1980Vol. 58(15), pp. 1596–1598
Citations Over TimeTop 15% of 1980 papers
Edward G. Janzen, Henry J. Stronks, Dale E. Nutter, Edward R. Davis, Henry N. Blount, J. Lee Poyer, Paul B. McCay
Abstract
Azidyl, cyanatyl, and cyanyl radicals and chlorine atoms have been detected by spin trapping using α-phenyl N-tert-butyl nitrone (PBN) in the monoelectronic electrooxidations of azide, cyanate, cyanide, and chloride. Azidyl and cyanatyl radicals were also detected with PBN in the persulfate oxidations of azide and cyanate. Azidyl radicals could be detected in the reaction of azide with hydroxyl radicals in the presence of PBN.
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