Transverse Dephasing Optimized Solid-State NMR Spectroscopy
Journal of the American Chemical Society2003Vol. 125(46), pp. 13938–13939
Citations Over TimeTop 10% of 2003 papers
Abstract
It is shown how coherence lifetimes in solid-state NMR experiments can be controlled. New decoupling schemes are introduced which actively optimize dephasing times, providing increases of up to a factor of 2 with respect to the best existing schemes. The new schemes are implemented in transverse-dephasing-optimized (TDOP) NMR experiments for the disorded solid cellulose, and for a microcrystalline protein, where sensitivity improvements of up to a factor of 5 are obtained.
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